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Author: search.filters.author.Chongsri, KrisanaSubject: search.filters.subject.Zinc oxide

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    Effect of F incorporation on physical and optical properties of hydrothermally grown ZnO nanorods
    (2018-01-01)
    Sinornate, Wuttichai
    ;
    Chongsri, Krisana
    ;
    Boonyarattanakalin, Kanokthip
    ;
    Pecharapa, Wisanu
    F-doped ZnO nanorods were synthesized via hydrothermal process with variation of Fluorine doping contents (0-10%) starting from zinc oxide thin film as a seeding layer for nanorod growth. The zinc oxide seeding thin film was prepared by sol-gel spin coating at 2000 rpm on glass substrate using zinc acetate precursor with annealing at 500°C in air for 2 h. Ammonium fluoride (NH<inf>4</inf>F) was used as F doping precursor. The properties of F-doped ZnO nanorods were characterized by field emission electron microscope (FESEM), X-ray diffraction (XRD), energy-dispersive X-ray spectroscopy (EDX) and UV-Visible spectrophotometer. Corresponding results indicated that growth of ZnO:F nanorods with good crystallinity and grown in (002) plane in undoped ZnO and F-doped ZnO 5%. The average size diameter of undoped and F-doped ZnO nanorods at 3%, 5% and 10% are 56, 96, 70 and 103 nm, respectively. From cross section images the average length of undoped and F-doped ZnO nanorods at 3%, 5% and 10% are 400, 375, 199 and 478 nm, respectively. The transmittance spectra shows moderate transparency (<80%) of the ZnO nanorod film in visible region with corresponding band gap range of 3.25-3.28 eV.
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    Hydrothermal synthesis and characterization of ZnO:F nanorod structure
    (2016-01-01)
    Sinornate, Wuttichai
    ;
    Chongsri, Krisana
    ;
    Pecharapa, Wisanu
    F-doped ZnO nanorod structures were synthesized via hydrothermal process with variation of doping content starting from zinc nitrate solution and zinc oxide thin film used as seeding layer. The zinc oxide seeding film was fabricated by spin coating on glass substrate using zinc acetate precursor and annealed at 500 °C for 2 h. Relevant properties of ZnO:F nanorod structures were characterized by scanning electron microscope (SEM), X-ray diffraction (XRD), energy-dispersive X-ray spectroscopy (EDX) and UV-VIS spectrophotometer. Corresponding results indicated that ZnO:F nanorod array, grown in (002) plane, has the characteristics of good crystallinity. In addition, this study showed that ZnO:F nanorod with exceptional structure can be obtained by hydrothermal process, operated at proper treatment time, temperature and F-doping content.