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Effect of a retrofitted metallic microfiber partial flow diesel particulate filter on a light duty diesel vehicle particle emission characteristics
(2024-02-01)
Mon Phyo, Mi Zwe
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Phairote, Watanyoo
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Srilomsak, Mek
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Charoenphonphanich, Chinda
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Masomtob, Manop
This study was conducted two distinct experiments, using a light-duty diesel vehicle at various engine speeds and loads as well as the new European driving cycle (NEDC) comparing commercial diesel fuel (B7) and pure biodiesel (B100). The NEDC involves a combination of urban and extra urban driving conditions. It aims to study a diesel vehicle's thermal efficiency as well as its gaseous and particulate matter (PM) emissions. This involves comparing results with and with no diesel oxidative catalyst (DOC) and a partial flow diesel particulate filter (PDPF) system. The surface morphology, micro- and nanostructure of a diesel vehicle's PM were also examined using scanning electron microscopy (SEM), transmission electron microscopy (TEM), energy dispersive spectroscopy (EDS), X-ray diffraction (XRD) and thermogravimetric analysis (TGA) to determine nanostructural and dimensional changes after mounting a DOC-PDPF system. Comparison of B7 and B100 combustion showed that B100 had around 1 % increase in brake thermal efficiency (BTE) at 1500 and 2000 rpm compared to B7 since B100 is a more oxygenated biofuel. At 2500 rpm, similar BTE values were observed. Introduction of a DOC-PDPF system resulted in an approximately 1 % BTE reduction for both fuels. This was due to greater friction losses caused by backpressure from the DOC-PDPF system. Increased exhaust backpressure was progressive, ranging from 1 kPa at idle speed to 6 kPa at high engine speeds for both tested fuels. The DOC-PDPF system respectively minimized PM emissions and particle numbers (PNs) by more than 50 % and 35 % for B7 and 71 % and 31 % for B100. These results are average values under the various phases of NEDC testing. A 30 % decrease in PM and a 44 % reduction in PNs under the overall test cycle were found when B100 was tested compared to B7. The soot primary particle size was reduced from 34.69 to 29.08 nm and the carbon fringe length diminished from 1.25 to 0.949 nm at different pre- and post-DOC-PDPF locations. This was due to partial oxidation on the surfaces of the PDPF metallic microstructure. PM undergoes simultaneous partial oxidation after passing through the DOC-PDPF system, as confirmed by TGA analysis.
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Experimental investigation of metallic partial-flow particulate filter on a diesel engine's combustion pressure and particle emission
(2023-09-01)
Mon Phyo, Mi Zwe
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Wai, Phyo
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Thin, Myat Hsu
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Oh, Ban Seok
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Phairote, Watanyoo
The study aims to present the combustion and exhaust behaviors of a 3 L, four-cylinder common rail diesel engine with three different kinds of conventional B7 diesel fuels with and without a platinum diesel oxidation catalyst (DOC) system and non-catalytic partial flow through a diesel particulate filter (P-DPF). Testing is performed under the three different operating conditions, idle to medium engine loading at 1000, 1500, and 2000 engine revolutions per minute with four different engine torques of 84, 112, 140 and 160 Nm. The surface morphology and agglomerate size of particulate matter (PM), single primary particle analysis as well as the fringe length of the carbon crystallite structure were also examined using scanning electron microscopy (SEM), transmission electron microscopy (TEM) and energy dispersive x-ray spectroscopy (EDS) to achieve a better understanding through image processing. The P-DPF system does not have a significant effect on an engine's in-cylinder combustion characteristics and brake thermal efficiency. The diesel engine's particle emissions are reduced by trapping them on the metallic micro-fibers of a P-DPF. CO<inf>2</inf>, NO, and O<inf>2</inf> levels show that the carbonaceous particle emissions on the micro-structure of the P-DPF passively react with NO<inf>2</inf> and O<inf>2</inf>. Consequently, diesel engine particle emissions can be reduced by around 50% using a P-DPF system under the experimental conditions of the current study.
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Physicochemical characterization of forest and sugarcane leaf combustion's particulate matters using electron microscopy, EDS, XRD and TGA
(2021-01-01)
Oo, Hay Mon
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Karin, Preechar
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Chollacoop, Nuwong
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Hanamura, Katsunori
Physical characteristics and quantitative elemental composition of PM and residual ash produced from sugarcane leaves (SCL) combustion were investigated using TEM-EDS compared with forest leaves (FRL). SEM-EDS was used to analyze the microstructure and chemical composition of biomass raw leaves and PM. XRD analysis was also performed to investigate the characterization of the crystalline nanostructure, structure of PM, and residual ash compared to the TEM image processing method. The oxidation kinetics of biomass raw materials, PM, and residual ash were investigated by TGA. The morphology of fine and ultrafine agglomerate structure of SCL soot and residual ash are not significantly different from the FRL soot and residual ash. The average diameter sizes of single primary nanoparticles of SCL and FRL soot are approximately 37 nm and 35 nm, while the sizes of residual ash are about 18 nm and 22 nm, respectively. The single primary nanoparticles of soot are mainly composed of curve line crystallites of carbon fringes, while residual ash is composed of straight-line lattice fringes. The average fringe lengths of SCL and FRL soot are about 1.25 nm and 1.04 nm from the outer shell and 0.89 nm and 0.74 nm from the inner core. The interlayer spacing of curve line carbon fringes of SCL and FRL soot is approximately 0.359 nm and 0.362 nm by the TEM image analysis and it was matched with XRD analysis. The biomass PMs are mainly composed of soot, Si, Ca, and K compounds: SiO<inf>2</inf>, CaCO<inf>3</inf>, and KCl.
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Impact of oil additive characteristics on biofuel engine wear using electron microscopy and confocal microscopy
(2019-01-01)
Rungsritanapaisan, Panyakorn
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Karin, Preechar
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Tanprayoon, Dhritti
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Tongsri, Ruangdaj
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Hanamura, Katsunori
Soot particles are produced during combustion process in the diesel engine. These particles will later exhaust into the thermosphere and part of them will contaminate the engine oil. When the lubricant is contaminated with soot, diesel engine abrasion or in a worst-case scenario lubricant starvation occurs. This situation will eventually lead into engine wear. High volume of soot also raises acid level of the area. If this state co-occurs with high temperature of the engine and volatile gases during operation, engine corrosion may also be produced. This research study the effect of additive volume on the dispersion of soot in engine oil and effect of additive on size and volume of soot which affect to mechanism of wear in metal by tribology four-ball tester, image analysis by scanning electron microscope and particle size analysis by laser diffraction technique.
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Morphology and oxidation kinetics of CI engine’s biodiesel particulate matters on cordierite Diesel Particulate Filters using TGA
(2017-02-01)
Karin, P.
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Boonsakda, J.
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Siricholathum, K.
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Saenkhumvong, E.
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Charoenphonphanich, C.
The impact of small compression ignition (CI) engine operation conditions and fuel properties on diesel and biodiesel particulate matters (PMs) quantity using opacity smoke meter is investigated. The biodiesel engine’s PMs are around a half of diesel engine PMs under the same engine operation conditions. Morphology of both engine’s PMs are also studied using a Scanning Electron Microscopy (SEM), Transmission Electron Microscopy (TEM) and image processing method. The average primary nanoparticle sizes of diesel and biodiesel engine’s PMs are approximately 34 nm and 32 nm, respectively. The result shows that engine operation condition and fuel property are strongly impact on the quantity and size distribution of primary nanoparticles emission. PM oxidation kinetics on conventional cordierite Diesel Particulate Filters (DPFs) powders by Thermo-gravimetric analysis (TGA) is also successfully studied. The calculated apparent activation energies of biodiesel engine’s PM oxidation on conventional cordierite DPFs powders are lower than that of diesel engine’s PM and carbon black because of unburned oxygenated molecule. The calculated apparent activation energy of biodiesel engine’s PM and diesel engine’s PM oxidize on conventional cordierite DPFs powders with pure air are in the range of 109 ~ 131 kJ/mole and 117 ~ 130 kJ/mole, respectively. It might be expected that smaller primary nanoparticle size of biodiesel engine’s PMs and bio-oxygenate unburned hydrocarbon can promote more PM oxidation rate during vehicle’s DPF regeneration process.
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Oxidation kinetics of small CI engine’s biodiesel particulate matter
(2015-04-01)
Karin, P.
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Borhanipour, M.
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Songsaengchan, Y.
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Laosuwan, S.
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Charoenphonphanich, C.
Particulate matters (PMs) oxidation kinetics by Thermo-gravimetric analysis (TGA) was successfully studied. The chemical content percentage of PM can be divided by oxidation temperature zoning in three main regions which are moisture, unburned hydrocarbon (HC) and carbon. It is clearly observed that the amount of each region is strongly depending on engine operating condition, the amount of unburned HC in low load condition of the engine load are larger than that of high load condition. The calculated apparent activation energies of biodiesel PM oxidation are lower than that of diesel PM and carbon black because of unburned oxygenated molecule. The calculated apparent activation energy of biodiesel and diesel PMs oxidize with air is in the range of 147–157 kJ/mole and 153–165 kJ/mole, respectively. The results of this research would be used as basic information for design and develop removing process of particulate matter emitted from engine combustion which using in diesel and biodiesel fuels.

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