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    Influence of ethanol-biodiesel blends on diesel engines combustion behavior and particulate matter physicochemical characteristics
    (2022-12-01)
    Karin, Preechar
    ;
    Tripatara, Aphichai
    ;
    Wai, Phyo
    ;
    Oh, Ban Seok
    ;
    Charoenphonphanich, Chinda
    Ethanol-blended biodiesel fuel can reduce smoke emissions by over 50% on both a single-cylinder engine and a four-cylinder engine. The average single primary particle size of biodiesel blended diesel, biodiesel, and ethanol blended biodiesel soot are approximately 30, 27, and 29 nm, respectively. The maximum graphene fringe length of biodiesel blended diesel, biodiesel, and ethanol blended biodiesel CI engine's soot are approximately 5.2, 4.6, and 4.5 nm. The carbon atom density of soot particles emitted from the diesel, biodiesel, and ethanol blended biodiesel CI engines are approximately 102, 91, and 88 atoms/nm3.
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    Impact of soot nanoparticle size and quantity on four-ball steel wear characteristics using EDS, XRD and electron microscopy image analysis
    (2022-01-01)
    Karin, Preechar
    ;
    Chammana, Pattara
    ;
    Oungpakornkaew, Pitchaporn
    ;
    Rungsritanapaisan, Panyakorn
    ;
    Amornprapa, Warawut
    The effect of soot contamination on the tribological performance of engine oil was investigated. Carbon black is introduced to simplify diesel engine soot contamination. Besides, the tribological performance issue is verified by a four-ball tribometer. The steel ball worn surfaces were studied by Scanning Electron Microscopy (SEM), Optical Microscope (OM) and Energy Dispersive X-ray spectroscopy (EDX). In addition, Transmission Electron Microscopy (TEM) was used to investigate the morphology and nanostructure of soot and carbon black. According to the four ball test results, the average wear scar diameter of steel ball tested with engine oil blended with N220, N330, N550 and N660 by 1% by weight is larger than that of pure engine oil by 26%, 38%, 41%, and 39%, respectively. The wear scar diameter tends to increase after blended larger size of carbon black particle. The steel balls tested with formulated engine oil without soot contamination and with soot contamination by 0.5 wt%, 1 wt%, and 2 wt% have average wear scar diameters of 621, 567, 784 and 894 nm, respectively. On the other hand, wear scar roughness of steel balls tested with formulated engine oil without soot contamination and with soot contamination by 0.5 wt%, 1 wt%, and 2 wt% were 2.28, 0.25, 1.49 and 1.76 μm, respectively. Consequently, quantity of the soot nanoparticle approximately 0.5% by mass in engine oil significantly plays an important role in steel ball wear scar diameter and surface roughness reduction. Moreover, the agglomerated soot which is larger than the oil film thickness might block the lubricant from entering the contact. It leads to the breakdown of the oil film thickness resulting in increasing adhesive wear on the worn surface.
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    Physicochemical Characterization of Diesel Engine’s Soot and Metal Oxide Ash Nanoparticles Using Electron Microscopy, EDS and TGA
    (2021-06-01)
    Karin, Preechar
    ;
    Koko, Phyozin
    ;
    Charoenphonphanich, Chinda
    ;
    Chollacoop, Nuwong
    ;
    Hanamura, Katsunori
    Physicochemical characteristics of metal oxide ash derived from engine oil additives on particulate matter (PM) from a diesel direct injection compression ignition (DDI-CI) engine, in terms of nanostructure and oxidation kinetics, were investigated through electron microscopy, energy dispersive X-ray spectroscopy and isothermal thermogravimetric analysis. Diesel and synthetic biodiesel were used as the baseline fuel. Engine performance and combustion characteristics of neat diesel and synthetic biodiesel fuel were initially reported. To enhance the formation of ash derived from lubricant additives, an accelerated ash loading method was used by dosing 10% by mass directly into the fuels. Different single primary particle nanostructures of soot and metal oxide ash were clearly observed. Single primary particle nanostructure of soot was a spherical shape composed of curve line carbon crystallites, while nanostructure of metal oxide ash was a spherically round outline shape comprised with parallel straight-line lattice fringes. Soot oxidation kinetics was significantly enhanced due to the presence of metal oxide ashes in the engine’s PM. In addition, the elemental analysis of metal oxide ash, derived from engine oil additives, was investigated using electron dispersive X-ray spectroscopy.