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Rapid detection of potassium sorbate in coconut water using near infrared hyperspectral imaging
(2026-01-01)
Tantinantrakun, Achiraya
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Kumpa, Benjaporn
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Ainkast, Pranpriya
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Thompson, Anthony Keith
;
Teerachaichayut, Sontisuk
Potassium sorbate may be illegally added to fresh coconut water in order to prolong its marketable life, but this adulteration may not be identified on the product label. The aim of this research was therefore to evaluate if samples of fresh coconut water that had been adulterated with measured amounts of potassium sorbate could be detected by near infrared hyperspectral imaging (NIR-HSI). Samples of coconut water with different potassium sorbate concentrations (N = 100) and pure coconut water samples (N = 100) were used in this study with their averaged spectral data used as independent variables. The smoothing spectral pretreatment gave the highest classification accuracy of 98.48% by partial least squares discriminant analysis (PLS-DA). While support vector machine regression (SVMR) with spectral pretreatment, using the 1st derivative combined with multiplicative scatter correction (MSC), achieved the optimum condition for developing the calibration model for determining potassium sorbate concentration with the correlation coefficient of prediction (R<inf>p</inf>) of 0.818 and the root mean square error of prediction (RMSEP) of 327.86 ppm. The results showed that NIR-HSI was able to be used as a fast, reliable, economic and environmentally friendly method of detecting potassium sorbate addition to coconut water.
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Near-infrared hyperspectral imaging for predicting the quality of SO2 pre-treated and dehydrated mango
(2025-08-01)
Aozora, Wayan Dipasasri
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Tantinantrakun, Achiraya
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Thompson, Anthony Keith
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Teerachaichayut, Sontisuk
Prediction for quality indices of SO<inf>2</inf> pre-treated and dehydrated mango was accessed by NIR-HSI. Models for predicting TSS and SO<inf>2</inf> content achieved R = 0.82; RMSEP = 2.42% and R = 0.83; RMSEP = 56.40 mg/kg, respectively. Visualization of TSS and SO<inf>2</inf> content could be presented by predictive images.
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Nondestructive evaluation of SW-NIRS and NIR-HSI for predicting the maturity index of intact pineapples
(2023-01-01)
Tantinantrakun, Achiraya
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Sukwanit, Supawan
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Thompson, Anthony Keith
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Teerachaichayut, Sontisuk
Determination of optimum maturity and ripeness of fruit is essential in the production of processed fruit, including pineapples, but this is difficult to achieve consistently by visual grading in commercial factories. Therefore, this study tested two nondestructive techniques for predicting the maturity index of intact pineapple. These were transmittance short wavelength near infrared spectroscopy (SW-NIRS) in the wavelength range of 665–955 nm and reflectance near infrared hyperspectral imaging (NIR-HSI) in the wavelength range of 935–1720 nm. The number of samples used for calibration was 120 for both SW-NIRS and NIR-HSI. The maturity index and spectral information of individual pineapple fruit were acquired from both techniques and analysed using the same procedure. Then, partial least squares regression (PLSR) was used to establish the models for predicting the maturity index of each intact fruit. The leave-one-out cross validation was used for evaluating the performance of the models. The results showed that both techniques gave reliable performance in predicting the maturity index of individual fruit, with a coefficient of determination considering cross validation (R<inf>cv</inf>2) for the prediction of the maturity index of 0.70 and a root mean square error in cross validation (RMSECV) of 2.16 when using SW-NIRS and R<inf>cv</inf>2 of 0.72 and RMSECV of 1.68 when using NIR-HSI. It was therefore concluded that both SW-NIRS and NIR-HSI had the potential for use in nondestructive analysis of the maturity of intact pineapple fruit in fruit processing factories.
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Prediction of water activity in mamón (Filipino sponge) cakes by near infrared hyperspectral imaging
(2020-01-01)
Sricharoonratana, Manunchaya
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Teerachaichayut, Sontisuk
Water activity in foods can result in detrimental microbial activity during storage. The usual methods of water activity measurement involve destruction of the sample. Near infrared (NIR) hyperspectral imaging has previously been successfully used as a non-destructive method to determine various physical and chemical characteristics of a variety of foods. Therefore, this method was tested to determine whether it could be used to measure water activity of mamón cakes, a popular sponge cake developed in the Philippines. Individual samples (n = 178) were divided into a calibration set (n=119) and a prediction set (n=59). These samples were tested using NIR hyperspectral imaging (935-1720 nm) with a smoothing spectral pretreatment selected for developing the calibration model. Partial least squares regression was used to establish the model in order to predict the water activity. The results showed the accuracy of the calibration model in prediction that gave a correlation coefficient of 0.767 and the root mean square error of prediction of 0.0130. It was therefore concluded that NIR hyperspectral imaging has a potential for use and application for measuring the water activity of mamón cakes.
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Grouping marian plums harvested at different times by transmittance near-infrared spectroscopy
(2017-11-25)
Teerachaichayut, S.
;
Phonmakham, S.
;
Suktanarak, S.
Marian plum (Bouea burmanica Griff.) ‘Toon Klaow’ is one of Thailand’s favorite fruits. Marian plum’s edible quality depends strongly on its harvest time. This study investigated a non-destructive technique for classifying marian plums according to their harvest time after the day that their blossom set. The non-destructive technique used was transmittance mode, short wavelength near-infrared (SW-NIR) spectroscopy in the wavelength range 660-960 nm. Marian plum samples (n=110) were harvested at 62, 65, 68 and 73 days after flowering. The soluble solids content (SSC) and titratable acid (TA) were determined accurately by standard methods. SW-NIR spectra of these samples were obtained and analyzed by principle component analysis (PCA) and partial least squares discriminant analysis (PLS-DA). The following spectral pretreatments were applied, standard normal variate (SNV), smoothing (Savitsky-Golay), and first derivative, in order to obtain optimal grouping results. The PC1 and PC2 score plot of the PCA could not clearly separate some of the classified groups. For the results of PLS-DA, its cross-validated grouping accuracy was R=0.91 and RMSECV=1.28; hence, it can be concluded that SW-NIR spectroscopy has good potential for determining the harvest time of marian plums.
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Non-destructive prediction of total soluble solids, titratable acidity and maturity index of limes by near infrared hyperspectral imaging
(2017-11-01)
Teerachaichayut, Sontisuk
;
Ho, Huong Thanh
This study was implemented for non-destructive prediction of total soluble solids (TSS), titratable acidity (TA) and calculation of TSS/TA as a measure of maturity index in intact limes using laboratory-based push-broom hyperspectral imaging (HSI) in reflectance mode in the range of 929–1671 nm. Limes were scanned by the HSI system in order to develop calibration models for predicting TSS, TA and TSS/TA using partial least square regression (PLSR). Original spectra obtained optimal conditions for establishing the models for TSS and TA while smoothing spectra for TSS/TA. The accuracy of the models for TSS, TA and TSS/TA provided coefficient of determination of prediction (R2<inf>p</inf>) of 0.838, 0.694 and 0.775, respectively and root mean square errors of prediction (RMSEP) of 0.237%, 0.288% and 0.049, respectively. Image processing algorithms were then built up by interpreting predictive values, from the models, to colors in each pixel of the images. The predictive visualization of TSS, TA and TSS/TA in all portions of the limes based on a color scale was presented. The results showed that the HSI technique has the capability of predicting TSS, TA and TSS/TA of intact limes non-destructively and the results could be visualized by different colors of the predictive images.
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Quantitative prediction of nitrate level in intact pineapple using Vis-NIRS
(2015-01-01)
Srivichien, Sasathorn
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Terdwongworakul, Anupun
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Teerachaichayut, Sontisuk
Before pineapples are canned, the ones with high nitrate level must be sorted out first because nitrate causes black stains on the surface of the can; therefore, a nondestructive technique for sorting out pineapples is clearly needed. The use of visible and near infrared (Vis-NIR) spectroscopy for such purpose was investigated in this study. A batch of 75 pineapple fruits that would have been delivered to a canning factory was tested. Spectra were acquired using a spectrophotometer in interactance mode with wavelengths in the region of 400-2500 nm. Twelve scans of different parts of each pineapple were made. The actual amount of nitrate in the pineapple flesh was determined by HPLC. Original spectra and pretreated spectra were both used to construct calibration models with partial least squares regression (PLSR). The best model was obtained from an average spectrum pretreated with first derivative treatment at the wavelength range of 600-1200 nm. Predictions based on this model matched closely with the actual nitrate contents, with a high correlation coefficient (R) of 0.95 and a low root mean square error of prediction (RMSEP) of 1.77 ppm. These results demonstrate that Vis-NIR spectroscopy can be used for rough screening of intact pineapple.
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Non-destructive detection of internal mold infection in sweet tamarind using short wavelength near infrared spectroscopy
(2014-10-20)
Teerachaichayut, S.
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Suktanarak, S.
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Kasemsumram, S.
Internal quality of sweet tamarind ('Prakaytong') is an essential commercial attribute. Determination of internal mold cannot be done by visual inspection on the outside of an intact tamarind. Therefore, a non-destructive measurement and data evaluation technique were considered using short wavelength near infrared (SW-NIR) transmittance spectroscopy in order to detect internal mold infection in sweet tamarind. A set of 176 tamarind samples (a calibration set = 124 and a prediction set = 52) were used in this research. Spectra in the region of 665-955 nm were acquired from scanning the center of each seed pod. The averaged spectral reading was used for partial least squares-discriminant analysis (PLS-DA) to establish a classification model for tamarind quality between groups of normal and defected samples. The calibration model obtained optimal result by cross validation using second derivative spectral pretreatment. The classification accuracy on the calibration set was 86.3% (58 out of 62 for the normal samples and 49 out of 62 for the defected samples) and on the prediction set was 84.6% (26 out of 26 for the normal samples and 18 out of 26 for the defected samples). The results showed that SW-NIR transmittance spectroscopy can be used to non-destructively detect internal mold infection in intact sweet tamarind.

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