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Rapid detection of potassium sorbate in coconut water using near infrared hyperspectral imaging
(2026-01-01)
Tantinantrakun, Achiraya
;
Kumpa, Benjaporn
;
Ainkast, Pranpriya
;
Thompson, Anthony Keith
;
Teerachaichayut, Sontisuk
Potassium sorbate may be illegally added to fresh coconut water in order to prolong its marketable life, but this adulteration may not be identified on the product label. The aim of this research was therefore to evaluate if samples of fresh coconut water that had been adulterated with measured amounts of potassium sorbate could be detected by near infrared hyperspectral imaging (NIR-HSI). Samples of coconut water with different potassium sorbate concentrations (N = 100) and pure coconut water samples (N = 100) were used in this study with their averaged spectral data used as independent variables. The smoothing spectral pretreatment gave the highest classification accuracy of 98.48% by partial least squares discriminant analysis (PLS-DA). While support vector machine regression (SVMR) with spectral pretreatment, using the 1st derivative combined with multiplicative scatter correction (MSC), achieved the optimum condition for developing the calibration model for determining potassium sorbate concentration with the correlation coefficient of prediction (R<inf>p</inf>) of 0.818 and the root mean square error of prediction (RMSEP) of 327.86 ppm. The results showed that NIR-HSI was able to be used as a fast, reliable, economic and environmentally friendly method of detecting potassium sorbate addition to coconut water.
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Assessing adulterated pineapple juice concentrate using electrical properties
(2025-01-01)
Tantinantrakun, Achiraya
;
Sinsamut, Varisara
;
Apairat, Nuengruthai
;
Smutrakalin, Thirapol
;
Thompson, Anthony Keith
The fraudulent addition of sugars to pineapple juice concentrate undermines consumer trust and satisfaction. Resistance (R), capacitance (C), dissipation factor (D), inductance (L), quality factor (Q), impedance (Z) and phase angle (θ) in the range of 0.012–200 kHz of juice adulterated with sugar increasing levels from 0 to 95% at 0.5% (w/w) intervals were tested to determine whether they could be used for detecting adulteration in pineapple juice concentrate using a LCR (inductance, capacitance, resistance) meter. A multiple linear regression (MLR) model was developed for predicting the concentration of additive sugars in samples. Linear discriminant analysis (LDA) was used for classifying pure pineapple juice concentrate and pineapple juice concentrate adulterated with added sugars. The most accuracy in the MLR model was obtained from θ, which achieved a correlation coefficient of prediction (R<inf>p</inf>) of 0.977 and a root mean square error of prediction (RMSEP) of 5.88% w/w. From the LDA analysis, the most accurate parameter for classification was C, which yielded a predictive classification accuracy of 94.57%. Therefore, this technique indicates its potential for use in the fruit juice industry a simple method for routinely testing in order to ensure the non-contamination of products offered for sale to consumers.
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Prediction of water activity in mamón (Filipino sponge) cakes by near infrared hyperspectral imaging
(2020-01-01)
Sricharoonratana, Manunchaya
;
Teerachaichayut, Sontisuk
Water activity in foods can result in detrimental microbial activity during storage. The usual methods of water activity measurement involve destruction of the sample. Near infrared (NIR) hyperspectral imaging has previously been successfully used as a non-destructive method to determine various physical and chemical characteristics of a variety of foods. Therefore, this method was tested to determine whether it could be used to measure water activity of mamón cakes, a popular sponge cake developed in the Philippines. Individual samples (n = 178) were divided into a calibration set (n=119) and a prediction set (n=59). These samples were tested using NIR hyperspectral imaging (935-1720 nm) with a smoothing spectral pretreatment selected for developing the calibration model. Partial least squares regression was used to establish the model in order to predict the water activity. The results showed the accuracy of the calibration model in prediction that gave a correlation coefficient of 0.767 and the root mean square error of prediction of 0.0130. It was therefore concluded that NIR hyperspectral imaging has a potential for use and application for measuring the water activity of mamón cakes.
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Detection of adulteration of tapioca starch with dolomite by near infrared hyperspectral imaging
(2020-01-01)
Khamsopha, Duangkamolrat
;
Teerachaichayut, Sontisuk
Tapioca starch adulterated with dolomite is sold in markets, but this adulteration cannot be identified by normal visual inspection. Near infrared (NIR) hyperspectral imaging has been successfully used as a non-destructive method of identifying various characteristics of food, therefore it was tested to identify dolomite adulteration. Adulterated tapioca starch samples were prepared by adding dolomite in the range of 0.5-100% (wt/wt). Samples (N=400) of pure tapioca starch (0) and adulterated tapioca starch (1) were divided into calibration set (N=300) and a prediction set (N=100). All samples were scanned using NIR hyperspectral imaging (935-1720 nm) and spectra were pre-processed using Savitzky-Golay first derivative differentiation pretreatment in order to obtain the optimal conditions for establishing a classification model. Partial least squares-discriminant analysis was carried out to evaluate the accuracy of classification tapioca starch adulterated with dolomite. The results showed the total accuracy of prediction for classification was 100%. Therefore, NIR hyperspectral imaging was demonstrated to have a potential for use in detecting adulteration of tapioca starch with dolomite.
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Non-destructive prediction of total soluble solids, titratable acidity and maturity index of limes by near infrared hyperspectral imaging
(2017-11-01)
Teerachaichayut, Sontisuk
;
Ho, Huong Thanh
This study was implemented for non-destructive prediction of total soluble solids (TSS), titratable acidity (TA) and calculation of TSS/TA as a measure of maturity index in intact limes using laboratory-based push-broom hyperspectral imaging (HSI) in reflectance mode in the range of 929–1671 nm. Limes were scanned by the HSI system in order to develop calibration models for predicting TSS, TA and TSS/TA using partial least square regression (PLSR). Original spectra obtained optimal conditions for establishing the models for TSS and TA while smoothing spectra for TSS/TA. The accuracy of the models for TSS, TA and TSS/TA provided coefficient of determination of prediction (R<sup>2</sup><inf>p</inf>) of 0.838, 0.694 and 0.775, respectively and root mean square errors of prediction (RMSEP) of 0.237%, 0.288% and 0.049, respectively. Image processing algorithms were then built up by interpreting predictive values, from the models, to colors in each pixel of the images. The predictive visualization of TSS, TA and TSS/TA in all portions of the limes based on a color scale was presented. The results showed that the HSI technique has the capability of predicting TSS, TA and TSS/TA of intact limes non-destructively and the results could be visualized by different colors of the predictive images.

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