Karin, Preechar

Preferred name

Karin, Preechar

Alternative Name

Karin, P.

Karin, Preecha

Main Affiliation

School of Engineering

preechar.ka@kmitl.ac.th

Now showing 1 - 10 of 35

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Physicochemical characteristics of ashes deposited on a wall flow diesel particulate filter of compression ignition engine
(2023-06-01)
Rodvanna, Sattatad
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Srilomsak, Mek
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Nuthong, Chaiwat
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Charoenphanich, Chinda
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Masomtob, Manop
The investigation of physicochemical characteristics of metal oxide ashes, deposited on a diesel particulate filter, was conducted using electron microscopy, energy dispersive spectroscopy, X-Ray fluorescence, and X-Ray diffractometry techniques. Iron is the main component of deposited ash on the DPF, and other ash components consisted of elements such as silicon, calcium, copper, sulfur, phosphorus, zinc, aluminum and minor chromium. It was clarified that this metal oxide ash has catalytic effect that contributed to an enhancement of soot oxidation. The apparent activation energies of soot oxidation on SiC powder and metal oxide ashes powder are approximately 169 and 135 kJ/mol, respectively.
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EFFECT OF BIODIESEL ON COMPRESSION IGNITION ENGINE’S COMBUSTION BEHAVIOR AND PARTICLE EMISSION
(2020-11-11)
Tripatara, A.
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Karin, P.
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Phairote, W.
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Charoenphonphanich, C.
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Masomtob, M.
Diesel Engines are widely known for a high compression ratio, which is proportional to the engine’s efficiency. The effect from direct injection of a diesel engine generates particulate matter (PM). PMs are mainly composed of Soot and Metallic Ash, which are harmful to human health. This research describes thermal efficiency, engine performance and combustion behavior at various load (20%, 50%, and 80%) and fuel (B7, B20, and B100) by using combustion pressure analyzer. The experimental results demonstrated that B100 has the highest ISFC and lowest ISEC for all test series owing to the highest indicated thermal efficiencies. Operating load and fuel are strongly proportional to heat release rate and ignition delay. The heat release rate of low load condition is retarded compare with medium and high load. Conventional diesel and biodiesel PMs were investigated by using Scanning electron microscopy (SEM) and Transmission electron microscopy (TEM). The average size of ultrafine particles that obtained from the experiment are range of 50-500 nm and primary nanoparticle size of B7 and B100 are in range of 25-50 nm.
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CHARACTERIZATION OF PARTICULATE MATTERS EMITTED FROM BIOMASS COMBUSTION USING ELECTRON MICROSCOPY AND ENERGY DISPERSIVE X-RAY SPECTROSCOPY
(2020-01-01)
Mon Oo, H.
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Karin, P.
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Masomtob, M.
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Saisirirat, P.
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Chollacoop, N.
Particulate Matters (PMs) emitted from biomass combustion including open burning of biomass agricultural residues, and forest fires must be reduced to protect both human health and the environment. The physical characteristics of morphology, elemental composition and nanostructure of particulate matters generated from biomass combustion were successfully investigated by using electron microscopy and energy dispersive X-ray spectroscopy (EDS) analysis with Scanning Electron Microscopy (SEM) and Transmission Electron Microscopy (TEM), and thermogravimetric analysis (TGA) was used to analyze the oxidation kinetics of particulate matters. Before biomass burning, it was found that about 65% of carbon fraction in biomass raw material while 95% of carbon fraction in soot and 84% in ash particles after burning. The average diameter size of single primary particles is approximately 36 nm. Nanostructure of the single primary particle of biomass soot is mainly composed of curve line carbon crystallites while metallic ash nanoparticle is composed of straight-line hatch patterns. The inter-planar spacing of fringes of biomass soot and ash crystallites is 0.36 nm and 0.28 nm, respectively. This article aims to study the different nanostructure of biomass forest leaves residual ash and soot such as agglomerated particles, primary particle's measurement using TEM image analysis.
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Physicochemical characterization of forest and sugarcane leaf combustion's particulate matters using electron microscopy, EDS, XRD and TGA
(2021-01-01)
Oo, Hay Mon
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Karin, Preechar
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Chollacoop, Nuwong
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Hanamura, Katsunori
Physical characteristics and quantitative elemental composition of PM and residual ash produced from sugarcane leaves (SCL) combustion were investigated using TEM-EDS compared with forest leaves (FRL). SEM-EDS was used to analyze the microstructure and chemical composition of biomass raw leaves and PM. XRD analysis was also performed to investigate the characterization of the crystalline nanostructure, structure of PM, and residual ash compared to the TEM image processing method. The oxidation kinetics of biomass raw materials, PM, and residual ash were investigated by TGA. The morphology of fine and ultrafine agglomerate structure of SCL soot and residual ash are not significantly different from the FRL soot and residual ash. The average diameter sizes of single primary nanoparticles of SCL and FRL soot are approximately 37 nm and 35 nm, while the sizes of residual ash are about 18 nm and 22 nm, respectively. The single primary nanoparticles of soot are mainly composed of curve line crystallites of carbon fringes, while residual ash is composed of straight-line lattice fringes. The average fringe lengths of SCL and FRL soot are about 1.25 nm and 1.04 nm from the outer shell and 0.89 nm and 0.74 nm from the inner core. The interlayer spacing of curve line carbon fringes of SCL and FRL soot is approximately 0.359 nm and 0.362 nm by the TEM image analysis and it was matched with XRD analysis. The biomass PMs are mainly composed of soot, Si, Ca, and K compounds: SiO<inf>2</inf>, CaCO<inf>3</inf>, and KCl.
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Oxidation Kinetics of Soot on Acicular Mullite Membrane Filter Using Electron Microscopy and Thermogravimetric Analysis
(2020-12-01)
Saenkhumvong, Eakkawut
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Karin, Preechar
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Charoenphonphanich, Chinda
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Vittayakorn, Naratip
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Hanamura, Katsunori
This paper investigates the oxidation kinetics of carbon black on acicular mullite using thermogravimetric (TGA) and mullite microstructures by scanning electron microscopy (SEM) for the development of diesel particulate filters (DPFs). It is observed that the amount of each chemical composition strongly affects the structure of mullite. The addition of AlF<inf>3</inf> and V<inf>2</inf>O<inf>5</inf> to mullite promotes the growth of needle-shaped mullite crystals. Thermogravimetric analysis was used to investigate and characterize chemical kinetics of soot oxidation for better understanding of designs and configurations of diesel particulate filters. The mass conversion of soot on the acicular mullite (ACM) is oxidized faster than that on the mullite (ML) membrane at all temperatures examined. The calculation of apparent activation energy (E<inf>a</inf>) of soot oxidation with isothermal methods on mullite was presented. The results showed that activation energy of soot oxidation is enhanced with ACM than with ML at all temperatures examined. The average calculated apparent activation energy of soot oxidation on ACM and ML are 146.4 kJ/mole and 155.3 kJ/mole, respectively.
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Physicochemical Characterization of Diesel Engine’s Soot and Metal Oxide Ash Nanoparticles Using Electron Microscopy, EDS and TGA
(2021-06-01)
Karin, Preechar
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Koko, Phyozin
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Charoenphonphanich, Chinda
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Chollacoop, Nuwong
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Hanamura, Katsunori
Physicochemical characteristics of metal oxide ash derived from engine oil additives on particulate matter (PM) from a diesel direct injection compression ignition (DDI-CI) engine, in terms of nanostructure and oxidation kinetics, were investigated through electron microscopy, energy dispersive X-ray spectroscopy and isothermal thermogravimetric analysis. Diesel and synthetic biodiesel were used as the baseline fuel. Engine performance and combustion characteristics of neat diesel and synthetic biodiesel fuel were initially reported. To enhance the formation of ash derived from lubricant additives, an accelerated ash loading method was used by dosing 10% by mass directly into the fuels. Different single primary particle nanostructures of soot and metal oxide ash were clearly observed. Single primary particle nanostructure of soot was a spherical shape composed of curve line carbon crystallites, while nanostructure of metal oxide ash was a spherically round outline shape comprised with parallel straight-line lattice fringes. Soot oxidation kinetics was significantly enhanced due to the presence of metal oxide ashes in the engine’s PM. In addition, the elemental analysis of metal oxide ash, derived from engine oil additives, was investigated using electron dispersive X-ray spectroscopy.
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Influence of ethanol-blended B7-diesel on in-cylinder combustion characteristic, engine thermal efficiency and emission of a 3L-compression ignition engine
(2026-03-01)
Suteerapongpun, Teerapat
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Thaeviriyakul, Poonnut
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Phairote, Watanyoo
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Saisirirat, Peerawat
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Po-ngaen, Watcharin
This study investigated the effects of blending weight ratio of 5% and 10% ethanol (B7E5 and B7E10) with standard B7-diesel on the performance, combustion, and emission characteristics of a light-duty common-rail diesel engine. The engine was tested on a dynamometer across various speeds (1600–2000 rpm) and loads (84 and 112 Nm) to analyze in-cylinder pressure, thermal efficiencies, and exhaust emissions. Results indicated significant emission benefits, especially at high loads. The B7E10 blend reduced smoke intensity by approximately 75% and carbon dioxide emissions by 34% compared to the baseline B7. The performance analysis revealed a critical trade-off associated with the ethanol blends: while the inherent oxygen content in ethanol significantly improved the indicated thermal efficiency (ITE) through enhanced combustion, its lower viscosity simultaneously led to increased frictional losses. Consequently, these competing effects resulted in only a modest improvement in brake thermal efficiency (BTE) and comparable brake-specific energy consumption (BSEC) compared to the baseline B7. The primary objective is to identify the benefits and trade-offs associated with ethanol blending in biodiesel-based diesel fuels that are compatible with existing diesel vehicles.
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Influence of V2O5 and AlF3 on Microstructure of Acicular Mullite Diesel Particulate Filter Along with Soot Oxidation Kinetics
(2021-12-01)
Saenkhumvong, Eakkawut
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Karin, Preechar
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Win, Swe Zin
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Sirivarocha, Settavit
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Chollacoop, Nuwong
In current research, aluminium oxide and silicon dioxide are used as raw materials for fabricating main structures of mullite diesel particulate filters. The variable substances applied to develop acicular mullite structure are titanium dioxide, aluminium fluoride, and vanadium oxide. Carbon black was used to create pores in mullite diesel particulate filters with 35 to 45% porosity based on the sintering temperature of 1300°C. The images of the filter’s porous surface microstructure were investigated using scanning electron microscopy. Vanadium oxide and aluminium fluoride play important roles in growth of acicular shape and acicular size for membrane, respectively. Acicular size of membrane varies from a hundred nano-meters to the submicron in needle diameter. The relation of all factors between pore size, porosity, surface roughness, and pin-shape microstructure can be controlled by additional amounts of additives. From Raman spectroscopy analysis, the soot formation of carbon black’s micro and nanostructure are acceptable to simulate diesel soot particles. In line with these results, carbon black was successfully used as a substitute of real engine soot in soot kinetics reactivity. In addition, the oxidation kinetics of soot particles on mullite and acicular mullite membrane were investigated by using tight contact in isothermal and loose contact in non-isothermal thermo-gravimetric analysis. The calculated apparent activation energies of soot oxidation with isothermal technique on mullite and acicular mullite membrane are approximately 213 and 141 kJ/mol while those values calculated with non-isothermal technique are 118 and 76 kJ/mol, respectively.
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Physicochemical characterization of direct injection Engines's soot using TEM, EDS, X-ray diffraction and TGA
(2021-06-01)
Oo, Hay Mon
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Karin, Preechar
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Charoenphonphanich, Chinda
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Chollacoop, Nuwong
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Hanamura, Katsunori
The physical characteristics and elemental composition of particulate matters (PMs) from gasoline direct injection spark ignition (GDI-SI) engines were successfully investigated using transmission electron microscopy - energy dispersive X-ray spectroscopy (TEM-EDS). Thermogravimetric analysis (TGA) was used to analyze the PMs oxidation. The morphology of agglomerated GDI-PMs is not significantly different from the diesel direct injection compression ignition (DDI-CI) engine's PMs. The spherical single primary nanoparticles of the engine's soot composed of curve line carbon crystallites. The average diameter size of the single primary nanoparticles of GDI, DDI, and carbon black are approximately 24 nm, 26 nm, and 31 nm, while the inter-planar spacing is about 0.364 nm, 0.358 nm, and 0.356 nm, respectively. The total fringe lengths of GDI, DDI, and carbon black are approximately 154 nm, 159 nm, and 163 nm measured from the areas of 10 nm × 10 nm inner core regions of primary nanoparticles, and are 180 nm, 195 nm, and 228 nm from the outer shell regions, respectively. The total fringe lengths of inner core are shorter than the outer shell. Besides, the engine's PMs contains both crystalline and amorphous carbon structure using XRD analysis. The GDI-PMs had the least crystalline structure compared to the DDI-PMs and carbon black due to the higher percentage of amorphous fraction. TGA analysis showed that the GDI-PMs oxidation was faster than the DDI-PMs and CB-N330 oxidation because of the primary particle size, the fringe length, and the crystal size which have an impact on oxidation kinetics of particulate matters.
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Influence of ethanol biodiesel blends on a diesel engine's efficiency and exhaust emission characteristics
(2022-01-01)
Kanokkhanarat, Phobkrit
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Karin, Preechar
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Depaiwa, Nattawoot
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Wongpattharaworakul, Veerayut
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Srisurangkul, Chadchai
The harm caused by polluted air occurs from dust, smoke, or soot. One of the main causes of pollutions is exhaust emission that comes from diesel engines of cars, trucks, buses, heavy machines, or generators for industrial because their thermal efficiency, torque, and performance are higher than the other engines. To reduce the emission from diesel engines, the fuel substitute for biodiesel which is made from based palm oil is one of the alternatives to use. So, the purpose of this paper is an experimental investigation of the engine performance, combustion characteristics, and smoke intensity of commercial biodiesel fuels (B10 and B20), pure biodiesel fuel (B100), and pure biodiesel blended with ethanol fuels (B100E5 and B100E10), which were performed at various loads (56, 84, 112, and 140Nm) and conducted at constant engine speeds (1000, 1500, and 2000 rpm). The experimental results show that pure biodiesel fuel (B100) and pure biodiesel blended with ethanol fuels (B100E5 and B100E10) have engine performance and combustion characteristics similar to commercial biodiesel fuels (B10 and B20). However, pure biodiesel fuels (B100) and pure biodiesel blended with ethanol fuels (B100E5 and B100E10) can reduce the emissions as the smoke intensity from commercial biodiesel (B10 and B20) is more than 50%.

Karin, Preechar

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