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  4. Semi-micro preparation and characterization of mesoporous silica microspheres from rice husk sodium silicate using a non-ionic surfactant as a template: Application in normal phase HPLC columns
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Semi-micro preparation and characterization of mesoporous silica microspheres from rice husk sodium silicate using a non-ionic surfactant as a template: Application in normal phase HPLC columns

Author(s)
Tungkananurak, Kanita
Kerdsiri, Sirinlux
Jadsadapattarakul, Damrongsak
Burns, Duncan Thorburn
Date Issued
July 1, 2007
Type
Article
DOI
10.1007/s00604-007-0743-x
Abstract
A simple and low-cost process has been developed for the production of mesoporous silica microspheres using a non-ionic surfactant as a template in an aqueous acidic sodium silicate solution prepared from rice husk. The influences of synthesis parameters such as the sodium silicate concentration, hydrochloric acid concentration, temperature and aging time on the morphology and on particle size range are described. The product's physical and normal phase chromatographic properties are reported. © 2007 Springer-Verlag.
Citation
Microchimica Acta, 159(3-4), 217-222, 2007
Subjects

Micelle

Normal phase

Rice husk

Silica microspheres

Sodium silicate

Triton X100 surfactan...

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