The effect of firing temperatures on (Pb0.75Ba 0.25)(Zr0.70Ti0.30)O3 ceramics prepared via the combustion technique

dc.contributor.authorSittiketkorn, Panadda
dc.contributor.authorWongtey, Pongkiti
dc.contributor.authorVittayakorn, Naratip
dc.contributor.authorBongkarn, Theerachai
dc.date.accessioned2026-08-06T10:07:54Z
dc.date.available2026-08-06T10:07:54Z
dc.date.issued2013-12-01
dc.description.abstractThe (Pb0.7<inf>5</inf>Ba0.2<inf>5</inf>)(Zr<inf>0.70</inf>Ti <inf>0.30</inf>)O<inf>3</inf> (PBZT) ceramics were prepared via the combustion technique. (CO(NH<inf>2</inf>)<inf>2</inf>) was used as a fuel. The effect of firing temperature on PBZT's phase formation, microstructure and electrical properties were investigated. The calcination and sintering temperatures were 600°C-1000°C and 1100°C-1300°C. The pure rhombohedral perovskite was obtained from the powders calcined at 850°C. The average particle size tended to increase with increased calcination temperatures. A pure rhombohedral perovskite phase was found in all pellet samples. The average grain size and linear shrinkage tended to increase from 0.57 to 2.15 μm and from 6.8 to 15.8% with increased sintering temperatures. The dielectric results indicated the relaxer behavior of PBZT ceramics. The Curie temperature tended to decrease with increasing sintering temperatures. The highest density (∼7.39 g/cm <sup>3</sup>) and highest dielectric constant (∼8620) were obtained by using the combustion technique which was higher than the conventional mixed oxide method. © 2013 Copyright Taylor and Francis Group, LLC.
dc.identifier.citationIntegrated Ferroelectrics, 149(1), 39-48, 2013
dc.identifier.doi10.1080/10584587.2013.852925
dc.identifier.issn10584587
dc.identifier.other2-s2.0-84891772046
dc.identifier.urihttps://dspace.kmitl.ac.th/handle/123456789/5223
dc.sourceIntegrated Ferroelectrics
dc.subjectcombustion technique
dc.subjectelectrical properties
dc.subjectLead barium zirconate titanate
dc.subjectmicrostructure
dc.subjectphase formation
dc.titleThe effect of firing temperatures on (Pb0.75Ba 0.25)(Zr0.70Ti0.30)O3 ceramics prepared via the combustion technique
dc.typeArticle

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