Synthesis and characterization of nanocrystalline manganese pyrophosphate Mn2P2O7

dc.contributor.authorBoonchom, Banjong
dc.contributor.authorBaitahe, Rattanai
dc.date.accessioned2026-08-06T09:58:46Z
dc.date.available2026-08-06T09:58:46Z
dc.date.issued2009-10-31
dc.description.abstractMn<inf>2</inf>P<inf>2</inf>O<inf>7</inf> polyhedral particles were synthesized by simple and cost-effective method using manganese nitrate hydrate and phosphoric acid in the presence of nitric acid with further calcinations at the temperature of 800 °C. The crystallite size obtained from X-ray line broadening is 31 ± 13 nm for the Mn<inf>2</inf>P<inf>2</inf>O<inf>7</inf>. The X-ray diffraction and SEM results indicated that the synthesized nanoparticles have only the structure without the presence of any other phase impurities. The FT-IR and FT-Raman spectra show characteristic bands of the P<inf>2</inf>O<inf>7</inf><sup>4-</sup> anion. The UV-Vis-NIR spectrum confirms the octahedral coordination of Mn<sup>2+</sup> ion. © 2009 Elsevier B.V. All rights reserved.
dc.identifier.citationMaterials Letters, 63(26), 2218-2220, 2009
dc.identifier.doi10.1016/j.matlet.2009.07.028
dc.identifier.issn0167577X
dc.identifier.other2-s2.0-69249230789
dc.identifier.urihttps://dspace.kmitl.ac.th/handle/123456789/2626
dc.sourceMaterials Letters
dc.subjectFTIR and FT-Raman
dc.subjectManganese pyrophosphate Mn2P2O7
dc.subjectNanoparticles
dc.subjectSynthesis
dc.titleSynthesis and characterization of nanocrystalline manganese pyrophosphate Mn2P2O7
dc.typeArticle

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