Pongampai, Satana

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Pongampai, Satana

satana.po@kmitl.ac.th

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Synergistic Piezo- and Triboelectricity in a Novel Triglycine Sulfate/Bacterial Cellulose/Chitosan Flexible Composite Nanogenerator
(2025-08-14)
Ukasi, Sirinya
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Saichompoo, Kittipan
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Sae-tang, Chanachot
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Pakawanit, Phakkhananan
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Pongampai, Satana
Organic piezoelectric materials offer sustainable alternatives for mechanical energy harvesting (MEH), yet their potential remains underexplored compared to inorganic counterparts. This study pioneers the use of triglycine sulfate (TGS), a rarely studied organic piezoelectric, within a flexible three-phase composite with bacterial cellulose (BC) and chitosan (CS) for piezoelectric (PENG) and triboelectric (TENG) nanogenerators. Unlike widely researched systems, TGS's unique hybrid organic–inorganic nature is leveraged here for the first time in MEH. Optimized at a 50:50 BC:CS ratio with 40 wt.% TGS, achieves a TENG output of 141.2 V and 93.3 µA post-poling—1.8 and 2.4 fold higher than unpoled samples—driven by TGS's dipole alignment. Separately, the configuration utilizing a 5 wt.% TGS loading yields 13.7 V and 0.19 µA. Advanced characterization (ATR-FTIR, SR-XTM) and simulations (COMSOL, DFT) reveal TGS's synergy with BC/CS roughness, enhancing charge generation. Delivering 118.65 µW cm−2, the TENG (from the 40 wt.% TGS poled sample) powers a digital watch, showcasing practical promise. This work not only introduces TGS as a novel MEH candidate but also provides mechanistic insights into its polarization, advancing bio-hybrid nanogenerator design.
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Towards the preparation of organic ferroelectric composites: fabrication of a gamma-glycine-bacterial cellulose composite via cold sintering process
(2023-07-01)
Noisak, Jitrawan
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Charoonsuk, Thitirat
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Pongampai, Satana
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Pinpru, Nattapong
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Pakawanit, Phakkhananan
The cold sintering process (CSP) has emerged as a revolutionary technique for low-temperature processing of ceramics and composites, enabling high-density fabrication at low temperatures. In this study, we demonstrated the implementation of CSP in fabricating the γ-glycine (γ-G)-bacterial cellulose (BC) composite and evaluated the effect of sintering temperature and holding time on the microstructure and electrical properties. Our findings revealed that an increase in sintering temperature and holding time leads to grain growth, as the transient solvent (water) facilitates the closely-packed microstructure. Moreover, the addition of BC as a filler into the γ-G matrix leads to a composite with a 10% increase in hardness when BC was uniformly distributed in γ-G. The composite with a relative density of 97% was successfully obtained at 120 °C/24 h, preserving the γ polymorph of glycine without the unwanted transformation commonly observed with traditional sintering. We also reported the dielectric and ferroelectric properties of the γ-G-BC composite, exhibiting a remanent polarization of 0.004 μC/cm2 and a coercive field of 1.201 kV/cm. Our findings suggest that CSP is a promising approach for low-temperature processing and fabrication of ceramics, especially when incorporating structurally sensitive filler such as organic ferroelectric, to achieve high-performance composites.
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Structural, optical, and electrical properties of cellulose/titanate nanosheets composite with enhanced protection against gamma irradiation
(2023-10-01)
Maluangnont, Tosapol
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Kwamman, Tanagorn
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Pulphol, Phieraya
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Pongampai, Satana
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Charoonsuk, Thitirat
Two-dimensional (2D) materials have emerged as a promising functional filler in nanocomposites due to their unique anisotropy and resilience to harsh conditions. We report herein the use of Ti<inf>0.91</inf>O<inf>2</inf> nanosheets as a protective component against γ-irradiation to cellulose paper. The titanate nanosheets were prepared via a sequence of solid-state synthesis of lepidocrocite-type Cs<inf>0.7</inf>Ti<inf>1.825</inf>O<inf>4</inf>, proton exchange to H<inf>0.7</inf>Ti<inf>1.825</inf>O<inf>4</inf>·H<inf>2</inf>O, and exfoliation with tetrabutylammonium hydroxide. The nanosheets were incorporated into the commercial cellulose filter paper by a simple dip coating up to 0.6 mg cm−2, equivalent to 10 wt% TiO<inf>2</inf>. The nanosheets distribution was demonstrated by energy dispersive X-ray (EDX) mapping, synchrotron radiation X-ray tomographic microscopy (SRXTM), and atomic force microscopy (AFM). It is found that γ-irradiation (up to 50 kGy) destroyed the cellulose Iβ crystallinity of uncoated paper, but this is less pronounced in the cellulose/titanate nanosheets composite. This was also confirmed by the lack of a 235 nm-absorption characteristics of irradiation-induced decomposition product(s) in nanosheets-containing papers, which also exhibit UVA shielding property. The coated samples remained white while the uncoated ones were darkened with γ-irradiation. In addition, the nanosheets-coated papers showed dielectric permittivity, loss tangent, and AC conductivity which were invariant of the γ-dose, unlike those from the uncoated ones. Our work demonstrates the use of lead-free Ti<inf>0.91</inf>O<inf>2</inf> nanosheets as a γ-shielding component to slow down/prevent structural, optical, and electrical properties damages in cellulose paper, which could extend to other nature-derived materials.
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DESIGNING WEAVING PATTERN AND ENGINEERING MULTILAYER STRUCTURE OF NYLON-ACRYLIC FABRIC UTILIZING IN TRIBOELECTRIC NANOGENERATOR
(2025-01-01)
Navatragulpisit, Suchanat
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Krailadsirirattna, Praophansupa
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Khwanming, Rawiwan
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Pongampai, Satana
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Plaipichit, Suwan
In the contemporary era, the textile triboelectric nanogenerator (T-TENG) has sparked interest to be a powerful energy supply for small electronic devices and electronic component in next generation of electronic textiles. Most T-TENG is developed by adding other materials to fabric or cloths that probably limit the comfortable use. Fabrication of conformable fabrics with high triboelectric outputs remains challenging. This research is firmly focused on the development of fully-fabric T-TENG by employing woven nylon-acrylic fabrics as the main contact material and designing a weaving pattern together with engineering a multi-layered structure to amplify its electrical efficiency. Based on the experimental results, different weaving patterns provided different electrical output values owing to its different contact surface areas. The matt weave pattern can yield the best electrical output regarding the extreme deformations. A further significant enhancement in T-TENG’s performance is consistent with inserting polymer intermediate layer. Adding ball-fiber and kapok serves as a synergetic charge-trapping interlayer, rendering a high triboelectricity of both open circuit voltage (VOC) and short circuit current (ISC) for 3 to 8 times higher than that of nylon-acrylic single layer. Finally, the multilayer fabric T-TENG is integrated with the long-sleeved garments and provide output enough to fully-charge the 0.22 μF and 0.33 μF capacitors together with brightening 30 LEDs. Finally, this work demonstrates a potential way with simple procedures in achieving fully-fabric T-TENG for small-scale energy sources that can harvest biomechanical energy to power electronic component for approaching the real application in E-textile systems.
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Simple Fabrication of Porous 3D Substrate Polydimethylsiloxane (PDMS) Composited with Polyvinylidene Fluoride-co-Hexafluoropropylene (PVDF-HFP) for Triboelectric Nanogenerator
(2022-01-01)
Pakawanit, Phakkhananan
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Pharino, Utchawadee
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Charoonsuk, Thitirat
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Sriphan, Saichon
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Pongampai, Satana
Owing to their structural advantages over bulk polymers, porous 3D substrates possess immense potential in triboelectric energy generation. This work reports the effective effort to fabricate the porous structure of polydimethylsiloxane, also known as the sponge-PDMS, by a simple template method. The sodium chloride salt from commodity product is used to create the 300 μm size of pores within the PDMS elastomeric layers, turning affects to the mechanical deformability of the triboelectric nanogenerator (TENG). The inner face of those pores is composited with the PVDF-HFP particles as a piezoelectric fillers. The presence of those fillers can be confirmed and their distribution within porous PDMS is 3D visualized by the synchrotron radiation X-ray tomography. The spatial distribution of the PVDF-HFP made it possible to fabricate the piezo-embedded macroporous TENG with high output power of 7.84 μW, giving over 2-fold enhancement, compared with the sponge-PDMS and even more when compared with the flat PDMS film under the same mechanical force.
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RARE EARTH OXIDE DIELECTRICS FOR FLEXIBLE TRIBOELECTRIC NANOGENERATOR
(2025-01-01)
Kingkam, Wilasinee
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Issarapanacheewin, Sudarat
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Ukasi, Sirinya
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Pulphol, Phieraya
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Pakawanit, Phakkhananan
Rare earth oxides (REO) are well known in catalysts, glass-related industries, and permanent magnets manufacturing for almost 70%, according to the mature industry. This work proposes the new developments of REO as the emergence for mechanical energy harvesting (MEH) technology. The binary-system of REO or R<inf>2</inf>O<inf>3</inf>, including La<inf>2</inf>O<inf>3</inf>, Sm<inf>2</inf>O<inf>3</inf> and Nd<inf>2</inf>O<inf>3</inf>, are used as dielectric materials to incorporate polydimethylsiloxane (PDMS) for fabricating flexible triboelectric nanogenerators (TENG), one of MEH devices. The change in REO’s amount was studied at 0.5, 2.5, 5, and 10 wt%. Upon applying mechanical force in vertical direction, the PDMS/R<inf>2</inf>O<inf>3</inf> TENG can convert mechanical energy into electricity for the best value of ~66 V and ~93 μA with power density of about ~62 μW·cm-2. The PDMS/La<inf>2</inf>O<inf>3</inf> can be used to fully charge the 0.22 and 0.33 μF capacitor within 3 seconds and power up over 100 LEDs directly. Moreover, the influence of triboelectric polarity and dielectricity on the triboelectric output performance is scientifically discussed by following the percolation point with air breakdown limitation’s theory. The researcher believes that the knowledge of this work will be inexhaustible useful to develop a group of REO in broad applications of MEH electronics in future.
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Synergistic Integration of MgAl-LDH Nanosheets into Bacterial Cellulose for High-Performance Triboelectric Nanogenerators
(2025-08-04)
Mohsom, Phitchayaphorn
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Suktep, Natdanai
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Sae-Tang, Chanachot
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Pongampai, Satana
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Pakawanit, Phakkhananan
A novel nanocomposite design is presented in which magnesium aluminum layered double hydroxide (MgAl-LDH) nanosheets are synergistically integrated with bacterial cellulose (BC) to fabricate a flexible triboelectric nanogenerator (TENG). Utilizing a facile solution synthesis combined with a casting process, composite films with controlled MgAl-LDH loadings (0.25–5% v/v) were developed. The optimal composite, containing 1.5% v/v MgAl-LDH, exhibits an open-circuit voltage (V<inf>OC</inf>) of 88.5 V, a short-circuit current (I<inf>SC</inf>) of 87.7 μA, and a maximum output power (P<inf>max</inf>) of 1250 μW (power density ≈138 μW/cm2), which is > 35 times higher than that of pristine BC. Notably, this performance corresponds to a superior filler efficiency metric, demonstrating a highly effective use of the nanosheet additive compared to other reported systems. This performance enhancement is attributed to the multifunctional role of MgAl-LDH nanosheets in increasing the dielectric constant through improved interfacial conductivity and the formation of parallel microcapacitors under an induced electric field. Finite element simulations corroborate the proposed mechanism, and practical demonstrations show the nanocomposite powering 200 LEDs as well as functioning as a self-powered sensor for finger movement monitoring. These findings advance the development of high-performance, flexible energy-harvesting devices.
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Simple enhanced charge density of chitosan film by the embedded ion method for the flexible triboelectric nanogenerator
(2022-12-01)
Charoonsuk, Thitirat
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Supansomboon, Supitcha
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Pakawanit, Phakkhananan
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Vittayakorn, Wanwilai
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Pongampai, Satana
This research proposed a simple ionic embedded method to improve electrical output performance by adding surface charges of cationic chitosan (CS) biopolymer for compatible utilization of the triboelectric nanogenerator (TENG). By simply embedding cationic salts, the TENG performance was enhanced by over four times more than that with pristine CS. Moreover, by modifying roughness on the film surface, the optimized condition of R-CS/3 %CaCl<inf>2</inf> reached the highest V<inf>OC</inf> and I<inf>SC</inf> of ~149 V and ~15 μA, respectively, thus exceeding the output from pristine R-CS TENG by four- and three times of ⁓38 V and ⁓5.1 μA. The maximum power output of 400 μW/cm2 can be observed at the 10 MΩ external load resistance. Finally, by integrating an automatic self-charge pumping (ASCP) module, the ASCP/CS-TENG provided highly efficient V<inf>OC</inf> and I<inf>SC</inf> output power by over 1.3 times more than the R-CS/3 %CaCl<inf>2</inf> TENG and could light up 72 light emitting diodes (LEDs) easily.
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Achieving a highly efficient chitosan-based triboelectric nanogenerator via adding organic proteins: Influence of morphology and molecular structure
(2021-11-01)
Charoonsuk, Thitirat
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Pongampai, Satana
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Pakawanit, Phakkhananan
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Vittayakorn, Naratip
The utilization of biodegradable materials for the triboelectric nanogenerator (TENG) has provoked intensive interest since the growth of electronic devices tended to operate in proximity of the human body. This work proposed highly efficient biopolymer, based on a chitosan (CS) TENG, by incorporating protein-based compounds as fillers. The effect of different types of protein; albumin, egg-shell membrane (ESM) and silk fiber (SF), with the loaded content on the output performance of TENG was explored. It was found that the output signal can be maintained and even enhanced by embedding interlaced-fiber and making a gauze-like structure inside the CS matrix. Morphologies not only have different types of amino acid side chains, but also affect triboelectric output performance. High content of glycine, alanine and serine consequently increases the output signal by providing additional charges from molecular polarizations. Mixing glycine amino acid in the presence of alanine and serine reduces the centrosymmetric structure of the host amino acid and creates polar domains. Adding SF in CS, therefore, achieves the best output voltage (V<inf>OC</inf>) and current (I<inf>SC</inf>) as compared to other additives. The CS/SF TENG, with 10 wt% SF added, can reach ~ 77 V and ~ 13 µA of V<inf>OC</inf> and I<inf>SC</inf>, respectively. Its maximum output power of ~ 202 μW, with power density of 22.4 μW/cm2, is 6 times higher than that from pristine CS TENG, which can easily light up 59 light emitting diodes (LEDs) connected in series. Finally, the biodegradability was confirmed at various weeks related to the output measurement of V<inf>OC</inf> and I<inf>SC</inf>. After 9 weeks of the soil burial test, the CS/SF still generated ~ 20 V V<inf>OC</inf> and ~ 2.5 µA I<inf>SC</inf> with 30% weight loss.
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Influence of pore morphologies on the mechanical and tribo-electrical performance of polydimethylsiloxane sponge fabricated via commercial seasoning templates
(2021-12-01)
Pharino, Utchawadee
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Sinsanong, Yoltawan
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Pongampai, Satana
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Charoonsuk, Thitirat
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Pakawanit, Phakkhananan
This work demonstrated the influence of pore morphologies on the mechanical behavior and tribo-electrical performance of fabricated polydimethylsiloxane (PDMS) sponge. Commercial seasonings with different 3D geometric shapes were used as a sacrificial template to control the pore structure of the PDMS sponge. The result indicated that the softest PDMS sponge was molded by using a sodium chloride (NaCl) crystal template, as indicated by the lowest compressive modulus value. Then, P(VDF–HFP) was incorporated into PDMS prepolymer in order to enhance the charge generation characteristic of PDMS. Besides, the composite 3D structure was revealed using synchrotron radiation X-ray tomographic microscopy (SRXTM). Interpretation from the SRXTM result confirmed that the porous structure had different pore shapes, i.e., an octahedral-like shape and a circular-like shape in a particular sponge. By pairing the composite PDMS sponge with an aluminum (Al) plate for the triboelectric nanogenerator (TENG), the maximum electrical outputs of ~29.9 V and ~0.56 μA for voltage and current, respectively, were detected with loading 50 wt% of P(VDF – HFP). The presented TENG was applied successfully for sensing basic human activities practically, which demonstrated potential applications in wearable electronics.

Pongampai, Satana

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